ISSN 2326-7283
African Journal of Internal Medicine ISSN 2326-7283 Vol. 7 (5), pp. 001-011, May, 2019. © International Scholars Journals
Full Length Research Paper
Synthesis and investigation of macro compounds via alkylation and azotation reactions
Nagham Mahmood Aljamali*, Radhiya A. Khdur and Haider Kareem Abd.
Chemistry Department, College of Education, Kufa University, Iraq.
Accepted 28 January, 2019
Abstract
This paper involved synthesis of series from macro compounds through reaction between di carbonyl compounds like (cyclo hexane-1,3-dione., 1,3-diphenyl–propadione, acetyl acetone, maleic anhydride, maleic acid, malonic acid) with di amine compounds or thiophene compound to produce compounds [1-5 ,7, 8,11], which reacted with azo compound, benzaldehyde, via alkylation reaction and azotation reaction to yield compounds [6,9,10,12] .The structure of these compounds were characterized by (H.NMR, FT.IR, C.H.N–analysis) techniques and their melting points.
Key words: Macro compound, azotation, seven–membered, thiophene, diazepine, hydrazo.